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Development of low-alloyed and rare-earth-free magnesium alloys having ultra-high strength
Pan HC; Qin GW; Huang YM; Ren YP; Sha XC; Han XD; Liu ZQ; Li CF; Wu XL(武晓雷); Chen HW; He C; Chai LJ; Wang YZ; Nie JF
发表期刊ACTA MATERIALIA
2018-05-01
卷号149页码:350-363
ISSN1359-6454
摘要Developing ultra-high strength in rare-earth-free Mg alloys using conventional extrusion process is a great challenge. What is even more difficult is to achieve such a goal at a lower processing cost. In this work, we report a novel low-alloyed Mg-2Sn-2Ca alloy (in wt. %) that exhibits tunable ultra-high tensile yield strength (360-440 MPa) depending on extrusion parameters. More importantly, there is little drop in mechanical properties of this alloy even when it is extruded at a speed several times higher than those used in the reported high strength Mg alloys. Examination of as-extruded microstructures of this Ca-containing Mg alloy reveals that the ultra-high strength is mainly associated with the presence of surprisingly submicron matrix grains (down to similar to 0.32 mu m). The results suggest that the Ca addition promotes accumulations of the pyramidal dislocations, which eventually transform into the low angular grain boundaries (LAGBs). The high number density of LAGBs separate the alpha-Mg matrix via either discontinuous dynamic recrystallization (DDRX) mechanism in the early stage or the continuous dynamic recrystallization (CDRX) mechanism in the later stage of extrusion, which effectively enhances the nucleation rates of the DRXed grains. More importantly, large amount of Ca segregation along LAGBs, accompanied with dynamically precipitated Mg2Ca nano-phases, are detected in the present non-severely deformed samples. It is the combination of solute segregations and numerous Mg2Ca nano-precipitates that contributes to the formation of the ultra-fine grains via pinning mechanism. The ultrafine grains size, Ca enrichment in most LAGBs, and residual Mg2Ca nano-precipitates would in turn contribute significantly to the enhancement of the yield strength of the as-extruded Mg-2Sn-2Ca (wt.%) alloy. The low content of alloying elements and the fast one-step extrusion process render the present alloys low-cost and thus have great potential in large-scale industry applications. (C) 2018 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
关键词Mg Alloy Mechanical Property Dynamic Recrystallization Segregation Strengthening Mechanism
DOI10.1016/j.actamat.2018.03.002
收录类别SCI ; EI
语种英语
WOS记录号WOS:000430895000031
关键词[WOS]SLOW-SPEED EXTRUSION ; ZN-ZR ALLOY ; CA-MN ALLOY ; MECHANICAL-PROPERTIES ; LOW-TEMPERATURE ; GRAIN-REFINEMENT ; MICROSTRUCTURE EVOLUTION ; MG-3AL-1ZN ALLOY ; PRISMATIC-SLIP ; PURE MAGNESIUM
WOS研究方向Materials Science ; Metallurgy & Metallurgical Engineering
WOS类目Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering
项目资助者National Key Research and Development Program of China(2016YFB0701200) ; National Natural Science Foundation of China(51525101 ; U1610253 ; 51371046 ; 51501032 ; 51131009)
论文分区一类
力学所作者排名5+
引用统计
被引频次:12[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://dspace.imech.ac.cn/handle/311007/77477
专题非线性力学国家重点实验室
推荐引用方式
GB/T 7714
Pan HC,Qin GW,Huang YM,et al. Development of low-alloyed and rare-earth-free magnesium alloys having ultra-high strength[J]. ACTA MATERIALIA,2018,149:350-363.
APA Pan HC.,Qin GW.,Huang YM.,Ren YP.,Sha XC.,...&Nie JF.(2018).Development of low-alloyed and rare-earth-free magnesium alloys having ultra-high strength.ACTA MATERIALIA,149,350-363.
MLA Pan HC,et al."Development of low-alloyed and rare-earth-free magnesium alloys having ultra-high strength".ACTA MATERIALIA 149(2018):350-363.
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