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High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures
Shen, Sijia1; Li, Hongbo1; Yang, Lingwei2; Li N(李娜)3; Wu, Jinting1; Zhao, Tingxing1
通讯作者Li, Hongbo(li-honggg@163.com) ; Yang, Lingwei(lingwei.yang@cardc.cn)
发表期刊POLYMER TESTING
2022-03-01
卷号107页码:8
ISSN0142-9418
摘要In this work, a novel high-throughput methodology based on combinations of nanoindentation, indentation creep and push-in methods, is proposed to measure in-situ the micro-mechanical properties of typical polymer matrix composites at a wide temperature range. The Young's modulus and strain rate sensitivity of a polyimide matrix and the interfacial shear strength in a quartz fiber reinforced polyimide matrix composite are measured at 25-350 degrees C for the first time. The results highlight a linear softening of the polyimide matrix at high temperatures, which is evidenced by the approximate linear decrease of Young's modulus from approximate to 5.0 GPa at 25 degrees C to approximate to 1.1 GPa at 350 degrees C. In comparison, the strain rate sensitivity of the polyimide matrix is increased, from approximate to 0.032 at 25 degrees C to approximate to 0.062 at 350 degrees C. This evidences a stronger visco-plasticity of polyimide at higher temperatures. The shear strength of the fiber/matrix interface is also temperature dependent. As the testing temperature increases from 25 to 300 degrees C, the shear strength is decreased from approximate to 147 MPa to approximate to 40 MPa. Specially, the interfacial strength is extremely low at 350 degrees C (approximate to 4 MPa), evidencing a failure of the composite at this temperature.
关键词Polyimide Nanoindentation Interface Micro-mechanics High temperature mechanics
DOI10.1016/j.polymertesting.2022.107483
收录类别SCI ; EI
语种英语
WOS记录号WOS:000765380600009
关键词[WOS]STRAIN-RATE SENSITIVITY ; SHEAR-STRENGTH ; PUSH-IN ; NANOINDENTATION ; BEHAVIOR ; TESTS
WOS研究方向Materials Science ; Polymer Science
WOS类目Materials Science, Characterization & Testing ; Polymer Science
资助项目National Natural Science Foundation of China[11902333]
项目资助者National Natural Science Foundation of China
论文分区一类
力学所作者排名3+
RpAuthorLi, Hongbo ; Yang, Lingwei
引用统计
被引频次:4[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://dspace.imech.ac.cn/handle/311007/88767
专题非线性力学国家重点实验室
作者单位1.Southwest Univ Sci & Technol, Sch Mat Sci & Engn, Mianyang 621000, Sichuan, Peoples R China;
2.China Aerodynam Res & Dev Ctr, Hyperveloc Aerodynam Inst, Mianyang 621000, Sichuan, Peoples R China;
3.Chinese Acad Sci, Inst Mech, LNM, Beijing 100190, Peoples R China
推荐引用方式
GB/T 7714
Shen, Sijia,Li, Hongbo,Yang, Lingwei,et al. High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures[J]. POLYMER TESTING,2022,107:8.
APA Shen, Sijia,Li, Hongbo,Yang, Lingwei,李娜,Wu, Jinting,&Zhao, Tingxing.(2022).High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures.POLYMER TESTING,107,8.
MLA Shen, Sijia,et al."High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures".POLYMER TESTING 107(2022):8.
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